2-Amino-3-nitro-9,10-anthracenedione

Base Information

• Chemical Name: 2-Amino-3-nitro-9,10-anthracenedione
• CAS No.: 56250-81-8
• Molecular Formula: C14H8N2O4
• Molecular Weight: 268.229
• Mol file: 56250-81-8.mol

Synonyms:2-Amino-3-nitro-9,10-anthracenedione

Chemical Property of 2-Amino-3-nitro-9,10-anthracenedione

Chemical Property:

• PSA: 105.98000
• LogP: 3.05680

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Amino-3-nitro-9,10-anthracenedione

There total 1 articles about 2-Amino-3-nitro-9,10-anthracenedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-acetamidoanthraquinone (3274-22-4) + nitric acid (7697-37-2,78989-43-2) → 2-acetylamino-1-nitro-anthraquinone (56250-79-4) + 2-amino-3-nitroanthraquinone (56250-81-8) + 2-amino-1-nitro-anthraquinone (10262-82-5)

Guidance literature:

at 15 - 20 ℃;

Reference yield:

2-amino-3-nitroanthraquinone (56250-81-8) → 2,3-diaminoanthracene (5227-67-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodiumsulfide nonahydrate / water / 1 h / 90 °C

2: zinc; copper(ll) sulfate pentahydrate; sodium hydroxide / water / 140 - 160 °C

With copper(ll) sulfate pentahydrate; sodiumsulfide nonahydrate; sodium hydroxide; zinc; In water;

DOI:10.1002/chem.201504453

Reference yield:

2-amino-3-nitroanthraquinone (56250-81-8) → 2,3-diphenylnaphtho[2,3-g]quinoxaline

Guidance literature:

Multi-step reaction with 3 steps

1: sodiumsulfide nonahydrate / water / 1 h / 90 °C

2: zinc; copper(ll) sulfate pentahydrate; sodium hydroxide / water / 140 - 160 °C

3: acetic acid / tetrahydrofuran / 0.5 h / 70 °C

With copper(ll) sulfate pentahydrate; sodiumsulfide nonahydrate; acetic acid; sodium hydroxide; zinc; In tetrahydrofuran; water;

DOI:10.1002/chem.201504453

upstream raw materials:

2-acetamidoanthraquinone

nitric acid

Downstream raw materials:

2,3-diaminoanthracene