bis(2-nitrobenzoic hydrazide)

Base Information

• Chemical Name: bis(2-nitrobenzoic hydrazide)
• CAS No.: 74415-18-2
• Molecular Formula: C₁₄H₁₀N₄O₆
• Molecular Weight: 330.257
• Mol file: 74415-18-2.mol

Synonyms:bis(2-nitrobenzoic hydrazide)

Chemical Property of bis(2-nitrobenzoic hydrazide)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(2-nitrobenzoic hydrazide)

There total 8 articles about bis(2-nitrobenzoic hydrazide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

o-nitrobenzohydrazide (606-26-8) → bis(2-nitrobenzoic hydrazide) (74415-18-2)

Guidance literature:

With copper diacetate; for 0.0833333h; microwave irradiation;

DOI:10.1081/SCC-120025183

Reference yield: 47.0%

2-nitrobenzyl chloride (610-14-0) → bis(2-nitrobenzoic hydrazide) (74415-18-2)

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; for 4h;

DOI:10.1039/P29800000773

Reference yield:

2-nitrobenzyl chloride (610-14-0) → bis(2-nitrobenzoic hydrazide) (74415-18-2) + o-nitrobenzohydrazide (606-26-8)

Guidance literature:

With hydrazine hydrate; benzene;

upstream raw materials:

3-(2-nitro-benzoylhydrazono)-butyric acid ethyl ester

2-nitrobenzyl chloride

o-nitrobenzohydrazide

methyl 2-nitrobenzoate

Downstream raw materials:

2-[5-(2-aminophenyl)-(1,3,4-oxadiazol-2-yl)]-benzenamine

2,2'-[1,3,4]thiadiazole-2,5-diyl-bis-aniline

diphenyl-[1,3,4]thiadiazole

2,5-bis-(phenyl)-1,3,4-oxadiazole

Refernces

• 1、 Mogilaiah,Anitha,Shiva Kumar,Shiva Prasad. "A convenient and simple transformation of acid hydrazides to N,N′-diacylhydrazines with Hg(OAc)2 under solid state conditions". experimental part. p. 126 - 128. Retrieved 2011/03/21.
• 2、 Prakash, Om,Sharma, Vijay,Sadana, Anil. "Hypervalent iodine oxidation of acid hydrazides: A new synthesis of N,N'-diacylhydrazines". . p. 3371 - 3377. Retrieved 2007/10/03.