Technology Process of 16-Methylheptadecan-1-ol
There total 12 articles about 16-Methylheptadecan-1-ol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylsilane; boron trifluoride diethyl etherate;
In
dichloromethane;
at 0 - 20 ℃;
for 0.75h;
Inert atmosphere;
DOI:10.3762/bjoc.9.210
- Guidance literature:
-
With
water; toluene-4-sulfonic acid;
In
methanol;
at 50 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.65 g / PPTS / CH2Cl2 / 3 h / 20 °C
2: dilithium tetrachlorocuprate / tetrahydrofuran / -10 - 0 °C
3: 330 mg / p-toluenesulphonic acid monohydrate; water / methanol / 2 h / 50 °C
With
dilithium tetrachlorocuprate; water; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; dichloromethane;
1: Addition / 2: coupling / 3: Hydrolysis;
