C₁₄H₁₆O₆

Base Information

• Chemical Name: C₁₄H₁₆O₆
• CAS No.: 1092835-48-7
• Molecular Formula: C₁₄H₁₆O₆
• Molecular Weight: 280.277
• Mol file: 1092835-48-7.mol

Synonyms:C₁₄H₁₆O₆

Chemical Property of C₁₄H₁₆O₆

Chemical Property:

Purity/Quality:

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Technology Process of C₁₄H₁₆O₆

There total 1 articles about C₁₄H₁₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C12H14Br2O4 + methyl chloroformate (79-22-1) → C14H16O6 (1092835-48-7)

Guidance literature:

C₁₂H₁₄Br₂O₄; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃;

methyl chloroformate; In tetrahydrofuran; hexane; at -78 - 0 ℃;

DOI:10.1021/ol802239n

Reference yield: 93.0%

C14H16O6 (1092835-48-7) + [3-[tert-butyl(dimethyl)silyl]oxy-4-methoxyphenyl]boronic acid (900152-53-6) → volubolin (89701-84-8)

Guidance literature:

C₁₄H₁₆O₆; [3-[tert-butyl(dimethyl)silyl]oxy-4-methoxyphenyl]boronic acid; With copper (I) acetate; In methanol; at 28 ℃; for 6h; Inert atmosphere;

With hydrogenchloride; In methanol; for 6h; Inert atmosphere; Reflux;

DOI:10.1021/ol802239n

upstream raw materials:

methyl chloroformate

Downstream raw materials:

volubolin

Refernces