sulfuric acid mono-(2-nitro-phenyl ester)

Base Information

• Chemical Name: sulfuric acid mono-(2-nitro-phenyl ester)
• CAS No.: 17396-91-7
• Molecular Formula: C₆H₅NO₆S
• Molecular Weight: 219.175
• Mol file: 17396-91-7.mol

Synonyms:sulfuric acid mono-(2-nitro-phenyl ester)

Chemical Property of sulfuric acid mono-(2-nitro-phenyl ester)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of sulfuric acid mono-(2-nitro-phenyl ester)

There total 2 articles about sulfuric acid mono-(2-nitro-phenyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-hydroxynitrobenzene (88-75-5,78813-12-4) → sulfuric acid mono-(2-nitro-phenyl ester) (17396-91-7)

Guidance literature:

With pyridine; sulfur trioxide; benzene;

DOI:10.1017/S0317167100001554

Reference yield:

trimethyl-sulfo-ammonium betaine (63147-26-2) + 2-hydroxynitrobenzene (88-75-5,78813-12-4) → sulfuric acid mono-(2-nitro-phenyl ester) (17396-91-7)

Guidance literature:

With sodium carbonate;

DOI:10.1002/jhet.5570390620

Reference yield:

sulfuric acid mono-(2-nitro-phenyl ester) (17396-91-7) → 2,2'-Dihydroxyazobenzene (2050-14-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium amalgam; water

2: hydrochloric acid / 70 °C

With hydrogenchloride; sodium amalgam; water;

DOI:10.1557/JMR.2000.0220

upstream raw materials:

trimethyl-sulfo-ammonium betaine

2-hydroxynitrobenzene

Downstream raw materials:

2,2'-Dihydroxyazobenzene