ethyl 4-[(2,2-dichloroacetyl)amino]-3-hydroxybanzoate

Base Information Edit

Chemical Name:ethyl 4-[(2,2-dichloroacetyl)amino]-3-hydroxybanzoate
CAS No.:852233-80-8
Molecular Formula:C₁₁H₁₁Cl₂NO₄
Molecular Weight:292.119
Hs Code.:
Mol file:852233-80-8.mol

Synonyms:ethyl 4-[(2,2-dichloroacetyl)amino]-3-hydroxybanzoate

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Chemical Property of ethyl 4-[(2,2-dichloroacetyl)amino]-3-hydroxybanzoate Edit

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of ethyl 4-[(2,2-dichloroacetyl)amino]-3-hydroxybanzoate

There total 3 articles about ethyl 4-[(2,2-dichloroacetyl)amino]-3-hydroxybanzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 79-36-7
dichloroacethyl chloride

: 87081-52-5
ethyl 4-amino-3-hydroxybenzoate

: 852233-80-8
ethyl 4-[(2,2-dichloroacetyl)amino]-3-hydroxybanzoate

Guidance literature:: With triethylamine; In diethyl ether; at -10 - 20 ℃; for 5h;
DOI:10.1021/jm048984g

Reference yield:

: 717-01-1
ethyl 3-hydroxy-4-nitro-benzoate

: 852233-80-8
ethyl 4-[(2,2-dichloroacetyl)amino]-3-hydroxybanzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / Pd/C / ethanol / 20 °C

2: 60 percent / triethylamine / diethyl ether / 5 h / -10 - 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In diethyl ether; ethanol;
DOI:10.1021/jm048984g

Reference yield:

: 619-14-7
3-hydroxy-4-nitro-benzoic acid

: 852233-80-8
ethyl 4-[(2,2-dichloroacetyl)amino]-3-hydroxybanzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / sulphuric acid / 2 h / Heating

2: 100 percent / H₂ / Pd/C / ethanol / 20 °C

3: 60 percent / triethylamine / diethyl ether / 5 h / -10 - 20 °C

With sulfuric acid; hydrogen; triethylamine; palladium on activated charcoal; In diethyl ether; ethanol;
DOI:10.1021/jm048984g