(3-Hydroxy-3-methylbutyl)triphenylphosphoniumbromid

Base Information Edit

Chemical Name:(3-Hydroxy-3-methylbutyl)triphenylphosphoniumbromid
CAS No.:67883-18-5
Molecular Formula:Br*C₂₃H₂₆OP
Molecular Weight:429.337
Hs Code.:
Mol file:67883-18-5.mol

Synonyms:(3-Hydroxy-3-methylbutyl)triphenylphosphoniumbromid

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Chemical Property of (3-Hydroxy-3-methylbutyl)triphenylphosphoniumbromid Edit

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Technology Process of (3-Hydroxy-3-methylbutyl)triphenylphosphoniumbromid

There total 2 articles about (3-Hydroxy-3-methylbutyl)triphenylphosphoniumbromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 35979-69-2
4-bromo-2-methyl-2-butanol

: 603-35-0
triphenylphosphine

: 67883-18-5
(3-Hydroxy-3-methylbutyl)triphenylphosphoniumbromid

Guidance literature:: In acetonitrile; for 24h; Heating;
DOI:10.1016/S0040-4039(00)01224-7

Reference yield:

: 558-30-5
2-methyl-1,2-epoxypropane

: 1779-49-3
Methyltriphenylphosphonium bromide

: 67883-18-5
(3-Hydroxy-3-methylbutyl)triphenylphosphoniumbromid

Guidance literature:: With phenyllithium; Yield given. Multistep reaction; 1.) THF, 15 min, 2.) THF, 5 min;
DOI:10.1021/jo00375a013

Reference yield: 84.0%

: 1160371-11-8
C₁₃H₂₄O₃

: 67883-18-5
(3-Hydroxy-3-methylbutyl)triphenylphosphoniumbromid

: C₁₈H₃₄O₃

Guidance literature:: (3-Hydroxy-3-methylbutyl)triphenylphosphoniumbromid; With methyllithium; In tetrahydrofuran; diethyl ether; at -20 - 20 ℃;

C₁₃H₂₄O₃; In tetrahydrofuran; diethyl ether; at -40 - 20 ℃;
DOI:10.1002/ejoc.200801183