Decanedioic acid butyl ester 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester

Base Information

• Chemical Name: Decanedioic acid butyl ester 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester
• CAS No.: 218899-30-0
• Molecular Formula: C₃₁H₄₂O₈
• Molecular Weight: 542.67
• Mol file: 218899-30-0.mol

Synonyms:Decanedioic acid butyl ester 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester

Chemical Property of Decanedioic acid butyl ester 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Decanedioic acid butyl ester 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester

There total 3 articles about Decanedioic acid butyl ester 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2'-hydroxy-4',6-dimethoxy-2-(p-methoxyphenyl)acetophenone (39604-68-7) + 9-Chlorocarbonyl-nonanoic acid butyl ester (218899-15-1) → Decanedioic acid butyl ester 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester (218899-30-0)

Guidance literature:

With pyridine; for 48h; Ambient temperature;

DOI:10.1055/s-1998-2221

Reference yield:

1,10-decanedioic acid (111-20-6,26776-29-4) → Decanedioic acid butyl ester 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester (218899-30-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 74 percent / Dowex 50W-X₂ / petroleum ether / 4.5 h / Heating

2: 83 percent / oxalyl chloride / 2 h / Heating

3: 65 percent / pyridine / 48 h / Ambient temperature

With pyridine; oxalyl dichloride; DOWEX 50W-X₂; In Petroleum ether;

DOI:10.1055/s-1998-2221

Reference yield:

Decanedioic acid monobutyl ester (5278-98-8) → Decanedioic acid butyl ester 3,5-dimethoxy-2-[2-(4-methoxy-phenyl)-acetyl]-phenyl ester (218899-30-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 83 percent / oxalyl chloride / 2 h / Heating

2: 65 percent / pyridine / 48 h / Ambient temperature

With pyridine; oxalyl dichloride;

DOI:10.1055/s-1998-2221

upstream raw materials:

2'-hydroxy-4',6-dimethoxy-2-(p-methoxyphenyl)acetophenone

9-Chlorocarbonyl-nonanoic acid butyl ester

1,10-decanedioic acid

Decanedioic acid monobutyl ester

Refernces