2,4,6-Trimethylaniline hydrochloride

Base Information

• Chemical Name: 2,4,6-Trimethylaniline hydrochloride
• CAS No.: 6334-11-8
• Molecular Formula: C9H13N•ClH
• Molecular Weight: 171.67
• European Community (EC) Number: 804-229-4
• NSC Number: 31
• UNII: 55G2955X2A
• DSSTox Substance ID: DTXSID6021400
• Mol file: 6334-11-8.mol

Synonyms:2,4,6-trimethylaniline;2,4,6-trimethylaniline hydrochloride;mesidine

Chemical Property of 2,4,6-Trimethylaniline hydrochloride

Chemical Property:

• Vapor Pressure: 0.0627mmHg at 25°C
• Melting Point: -5oC
• Boiling Point: 231.3°C at 760 mmHg
• Flash Point: 96.1°C
• PSA: 26.02000
• LogP: 3.57720
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 171.0814771
• Heavy Atom Count: 11
• Complexity: 99.3

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=CC(=C(C(=C1)C)N)C.Cl

Technology Process of 2,4,6-Trimethylaniline hydrochloride

There total 3 articles about 2,4,6-Trimethylaniline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2,4,6-trimethylaniline (88-05-1) → 2,4,6-trimethylaniline hydrochloric acid salt (6334-11-8)

Guidance literature:

With hydrogenchloride; In diethyl ether; at 0 - 20 ℃; for 0.5h;

Reference yield:

→ 2,4,6-trimethylaniline hydrochloric acid salt (6334-11-8) + 1,2-bis(2',4',6'-trimethylphenyl-amino)-propane dihydrochloride

Guidance literature:

Reference yield:

azidotri-2,4,6-trimethylphenylgermane (124862-47-1) → dichlorodimesitylgermane (96481-42-4) + Ge(C6H2(CH3)3)2NHCH2(C6H2(CH3)2) (124862-48-2) + 2,4,6-trimethylaniline hydrochloric acid salt (6334-11-8)

Guidance literature:

With hydrogenchloride; byproducts: N2; Irradiation (UV/VIS); irradiation, react. with HCl;

DOI:10.1016/0022-328X(90)80264-Z

upstream raw materials:

2,4,6-trimethylaniline

azidotri-2,4,6-trimethylphenylgermane

Downstream raw materials:

Mesityl-guanidin

2,4,6-trimethylphenyl diazonium chloride

N-(2,4,6-trimethylphenyl)imidazole

N-(2,4,6-trimethyl-phenyl)-guanidine hydrochloride

Refernces

• 1、 Riviere-Baudet, M.,Satge, J.,Morere, A.. "N-Mesityl dimesitylgerma-imine". . p. C7 - C11. Retrieved 2007/10/02.