C₁₃H₁₄N₂O₂

Base Information Edit

Chemical Name:C₁₃H₁₄N₂O₂
CAS No.:128366-51-8
Molecular Formula:C₁₃H₁₄N₂O₂
Molecular Weight:230.266
Hs Code.:
Mol file:128366-51-8.mol

C<sub>13</sub>H<sub>14</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₃H₁₄N₂O₂

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Chemical Property of C₁₃H₁₄N₂O₂ Edit

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Technology Process of C₁₃H₁₄N₂O₂

There total 14 articles about C₁₃H₁₄N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1240244-31-8
C₁₇H₂₁N₃O₂

: 128366-51-8
C₁₃H₁₄N₂O₂

Guidance literature:: With hydrogenchloride; hydrogen; palladium 10% on activated carbon; In water; at 85 ℃; for 21h; under 2844.39 Torr; Inert atmosphere; Sealed bottle;

Reference yield:

: 83647-43-2
3-bromo-2-methylbenzyl alcohol

: 128366-51-8
2-methyl-3-(1'-methyl-1'-(5''-imidazolyl)methyl)benzoic acid

Guidance literature:: Multi-step reaction with 8 steps

1: 75 percent / 1.) NaH / dimethylformamide / 1.) 0 deg.C, 30 min, 2.) 30 deg.C, 3 h

2: 1.) Mg / 1.) THF, reflux, 2.5 h, 2.) THF, reflux 3 h

3: 82 percent / pyridinium chlorochromate / CH₂Cl₂ / 36 h / 25 °C

4: 90 percent / tetrahydrofuran / 1.) -78 deg. C, 1 h, 2.) -78 - 0 deg.C, 1 h

5: 100 percent / phosphoryl chloride / CH₂Cl₂ / 1 h / 25 °C

6: 91 percent / H₂ / 10percent Pd/C / ethyl acetate / 48 h / 3102.9 Torr

7: 68 percent / DDQ / CH₂Cl₂ / 1 h

8: tetra-n-butylamonium permanganate, pyridine / 1 h / 25 °C

With pyridine; tetra-n-butylammonium permanganate; hydrogen; sodium hydride; magnesium; pyridinium chlorochromate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570300631

Reference yield:

: 529-20-4
2-methylphenyl aldehyde

: 128366-51-8
2-methyl-3-(1'-methyl-1'-(5''-imidazolyl)methyl)benzoic acid

Guidance literature:: Multi-step reaction with 9 steps

1: 1.) AlCl₃, Br₂, 2.) NaBH₄ / 1.) CH₂Cl₂, 40 deg.C, 30 min, 2.) CH₃OH, 0 deg.C, 2 h

2: 75 percent / 1.) NaH / dimethylformamide / 1.) 0 deg.C, 30 min, 2.) 30 deg.C, 3 h

3: 1.) Mg / 1.) THF, reflux, 2.5 h, 2.) THF, reflux 3 h

4: 82 percent / pyridinium chlorochromate / CH₂Cl₂ / 36 h / 25 °C

5: 90 percent / tetrahydrofuran / 1.) -78 deg. C, 1 h, 2.) -78 - 0 deg.C, 1 h

6: 100 percent / phosphoryl chloride / CH₂Cl₂ / 1 h / 25 °C

7: 91 percent / H₂ / 10percent Pd/C / ethyl acetate / 48 h / 3102.9 Torr

8: 68 percent / DDQ / CH₂Cl₂ / 1 h

9: tetra-n-butylamonium permanganate, pyridine / 1 h / 25 °C

With pyridine; sodium tetrahydroborate; aluminium trichloride; tetra-n-butylammonium permanganate; hydrogen; bromine; sodium hydride; magnesium; pyridinium chlorochromate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570300631