C₂₁H₃₀N₂O₇

Base Information

• Chemical Name: C₂₁H₃₀N₂O₇
• CAS No.: 1361249-81-1
• Molecular Formula: C₂₁H₃₀N₂O₇
• Molecular Weight: 422.478
• Mol file: 1361249-81-1.mol

Synonyms:C₂₁H₃₀N₂O₇

Chemical Property of C₂₁H₃₀N₂O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₂₁H₃₀N₂O₇

There total 1 articles about C₂₁H₃₀N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

Boc-D-Phg-OH (33125-05-2) + 5-amino-5-deoxy-1,2-O-isopropylidene-a-D-xylofuranose (4613-58-5,25531-86-6,25572-88-7) → C21H30N2O7 (1361249-81-1)

Guidance literature:

Boc-D-Phg-OH; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at -15 ℃; Inert atmosphere;

5-amino-5-deoxy-1,2-O-isopropylidene-a-D-xylofuranose; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/adsc.201100766

Reference yield: 64.0%

C21H30N2O7 (1361249-81-1) + benzoyl chloride (98-88-4) → C28H34N2O8 (1361249-99-1)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/adsc.201100766

Reference yield:

C21H30N2O7 (1361249-81-1) → C28H34N2O7S (1361250-21-6)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: Lawessons reagent / tetrahydrofuran / 60 °C / Inert atmosphere

With Lawessons reagent; pyridine; In tetrahydrofuran; dichloromethane;

DOI:10.1002/adsc.201100766

upstream raw materials:

Boc-D-Phg-OH

5-amino-5-deoxy-1,2-O-isopropylidene-a-D-xylofuranose

Downstream raw materials:

C₂₈H₃₄N₂O₇S

C₂₈H₃₄N₂O₈

Refernces