2-Propenoic acid, 3-(4-aminophenyl)-, hydrochloride

Base Information

• Chemical Name: 2-Propenoic acid, 3-(4-aminophenyl)-, hydrochloride
• CAS No.: 54057-95-3
• Molecular Formula: C9H9 N O2 . Cl H
• Molecular Weight: 199.637
• Hs Code.: 2922499990
• Mol file: 54057-95-3.mol

Synonyms:4-AMINOCINNAMIC ACID HCl;EINECS 258-940-4;2-Propenoic acid, 3-(4-aminophenyl)-, hydrochloride;p-AMINOCINNAMIC ACID HYDROCHLORIDE;C9H9NO2.ClH;C9-H9-N-O2.Cl-H;2-Propenoic acid, 3-(4-aminophenyl)-, hydrochloride (1:1);Para-aminocinnamic acid hydrochloride;FT-0640217

Chemical Property of 2-Propenoic acid, 3-(4-aminophenyl)-, hydrochloride

Chemical Property:

• Vapor Pressure: 2.13E-06mmHg at 25°C
• Melting Point: 265-270 °C (dec.)(lit.)
• Boiling Point: 378.4°Cat760mmHg
• Flash Point: 182.6°C
• PSA: 63.32000
• Density: g/cm³
• LogP: 2.74980
• Storage Temp.: Sealed in dry,Room Temperature
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 199.0400063
• Heavy Atom Count: 13
• Complexity: 181

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-AminocinnamicAcidHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1=CC(=CC=C1C=CC(=O)O)N.Cl

Technology Process of 2-Propenoic acid, 3-(4-aminophenyl)-, hydrochloride

There total 2 articles about 2-Propenoic acid, 3-(4-aminophenyl)-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

p-azidocinnamic acid (30980-75-7) → 3-(p-aminophenyl)propenoic acid hydrochloride (54057-95-3)

Guidance literature:

With hydrazinium monoformate; zinc; In methanol; at 20 ℃; for 0.166667h;

Reference yield:

p-aminocinnamic acid (2393-18-2) → 3-(p-aminophenyl)propenoic acid hydrochloride (54057-95-3)

Guidance literature:

With hydrogenchloride; In acetone;

DOI:10.1021/acs.macromol.6b00220

Reference yield:

3-(p-aminophenyl)propenoic acid hydrochloride (54057-95-3) → 4,4'-diaminotruxillate dihydrochloride

Guidance literature:

In hexane; UV-irradiation;

DOI:10.1021/acs.macromol.6b00220

upstream raw materials:

p-azidocinnamic acid

p-aminocinnamic acid

Refernces

• 1、 Tateyama, Seiji,Masuo, Shunsuke,Suvannasara, Phruetchika,Oka, Yuuki,Miyazato, Akio,Yasaki, Katsuaki,Teerawatananond, Thapong,Muangsin, Nongnuj,Zhou, Shengmin,Kawasaki, Yukie,Zhu, Longbao,Zhou, Zhemin,Takaya, Naoki,Kaneko, Tatsuo. "Ultrastrong, Transparent Polytruxillamides Derived from Microbial Photodimers". . p. 3336 - 3342. Retrieved 2016.