2,2'-disulfanediyl-di-benzoic acid bis-benzenesulfonylamide

Base Information

• Chemical Name: 2,2'-disulfanediyl-di-benzoic acid bis-benzenesulfonylamide
• CAS No.: 177786-68-4
• Molecular Formula: C₂₆H₂₀N₂O₆S₄
• Molecular Weight: 584.719
• Mol file: 177786-68-4.mol

Synonyms:2,2'-disulfanediyl-di-benzoic acid bis-benzenesulfonylamide

Chemical Property of 2,2'-disulfanediyl-di-benzoic acid bis-benzenesulfonylamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2'-disulfanediyl-di-benzoic acid bis-benzenesulfonylamide

There total 3 articles about 2,2'-disulfanediyl-di-benzoic acid bis-benzenesulfonylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(phenylsulfonyl)benzo[d]isothiazol-3(2H)-one (17927-88-7) → 2,2'-disulfanediyl-di-benzoic acid bis-benzenesulfonylamide (177786-68-4)

Guidance literature:

With pyridine;

DOI:10.1039/jr9470001574

Reference yield:

2,2'-dithiodibenzoic acid dichloride (19602-82-5) → 2,2'-disulfanediyl-di-benzoic acid bis-benzenesulfonylamide (177786-68-4)

Guidance literature:

Multi-step reaction with 2 steps

2: zinc; aqueous hydrochloric acid; acetic acid / und anschliessenden Behandeln mit Eisen(III)-chlorid

With hydrogenchloride; acetic acid; zinc;

DOI:10.1039/jr9390000760

Reference yield:

benzenesulfonamide (98-10-2) → 2,2'-disulfanediyl-di-benzoic acid bis-benzenesulfonylamide (177786-68-4)

Guidance literature:

Multi-step reaction with 2 steps

2: zinc; aqueous hydrochloric acid; acetic acid / und anschliessenden Behandeln mit Eisen(III)-chlorid

With hydrogenchloride; acetic acid; zinc;

DOI:10.1039/jr9390000760

upstream raw materials:

2-(phenylsulfonyl)benzo[d]isothiazol-3(2H)-one

2,2'-dithiodibenzoic acid dichloride

benzenesulfonamide

Downstream raw materials:

[2-(1-acetyl-2-oxo-propylsulfanyl)-benzoyl]-benzenesulfonyl-amine

benzenesulfonamide

2-acetyl-3-hydroxybenzo[b]thiophene