Technology Process of C17H18N2O6
There total 5 articles about C17H18N2O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 0 - 20 ℃;
for 18h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine / acetonitrile / 24 h / 0 - 20 °C / Inert atmosphere
2.1: triethylamine / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere
3.1: dimethyl sulfoxide / 21 h / 80 °C / Inert atmosphere
4.1: hydrogenchloride; water / 4.5 h / Reflux
4.2: 7 h / 0 - 20 °C
4.3: pH 2
5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
dichloromethane; dimethyl sulfoxide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere
2.1: dimethyl sulfoxide / 21 h / 80 °C / Inert atmosphere
3.1: hydrogenchloride; water / 4.5 h / Reflux
3.2: 7 h / 0 - 20 °C
3.3: pH 2
4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
dichloromethane; dimethyl sulfoxide;
