N'-benzoyl-N,N'-bis(2,6-dimethylphenyl)anthranilamide

Base Information

• Chemical Name: N'-benzoyl-N,N'-bis(2,6-dimethylphenyl)anthranilamide
• CAS No.: 86365-68-6
• Molecular Formula: C₃₀H₂₈N₂O₂
• Molecular Weight: 448.565
• Mol file: 86365-68-6.mol

Synonyms:N'-benzoyl-N,N'-bis(2,6-dimethylphenyl)anthranilamide

Chemical Property of N'-benzoyl-N,N'-bis(2,6-dimethylphenyl)anthranilamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N'-benzoyl-N,N'-bis(2,6-dimethylphenyl)anthranilamide

There total 3 articles about N'-benzoyl-N,N'-bis(2,6-dimethylphenyl)anthranilamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2,6-dimethylphenyl)-3-<(2,6-dimethylphenyl)amino>-2-phenylindole (86365-67-5) → N'-benzoyl-N,N'-bis(2,6-dimethylphenyl)anthranilamide (86365-68-6)

Guidance literature:

With chromium(VI) oxide; In acetic acid; at 80 ℃; for 0.166667h;

DOI:10.1021/jo00165a028

Reference yield:

N-(2,6-dimethylphenyl)anthranilic acid (18201-61-1) → N'-benzoyl-N,N'-bis(2,6-dimethylphenyl)anthranilamide (86365-68-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 48percent HBr / 2 h / Heating

2: 67 percent / 4-toluenesulfonic acid / 12 h / Heating

3: 3.0 g / CrO₃ / acetic acid / 0.17 h / 80 °C

With chromium(VI) oxide; hydrogen bromide; toluene-4-sulfonic acid; In acetic acid;

DOI:10.1021/jo00165a028

Reference yield:

2,6-dimethylaniline (87-62-7) → N'-benzoyl-N,N'-bis(2,6-dimethylphenyl)anthranilamide (86365-68-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 67 percent / 4-toluenesulfonic acid / 12 h / Heating

2: 3.0 g / CrO₃ / acetic acid / 0.17 h / 80 °C

With chromium(VI) oxide; toluene-4-sulfonic acid; In acetic acid;

DOI:10.1021/jo00165a028

upstream raw materials:

1-(2,6-dimethylphenyl)-3-<(2,6-dimethylphenyl)amino>-2-phenylindole

N-(2,6-dimethylphenyl)anthranilic acid

2,6-dimethylaniline

Downstream raw materials:

N-phenyl-2,6-dimethylaniline

benzoic acid

2,6-dimethylaniline

Refernces