Technology Process of Manganese(III) 2,4-pentanedionate
There total 9 articles about Manganese(III) 2,4-pentanedionate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tert-butylammonium hexafluorophosphate(V);
In
acetylacetone;
Electrochem. Process; tetra-n-butylammonium hexafluorophosphate added to dry acetylacetone, Mnelectrode; evapn. under vac., residue washed twice with hexane and twice with petroleum ether;
DOI:10.1080/15533170701748548
- Guidance literature:
-
In
water;
for 0.25h;
Heating / reflux;
- Guidance literature:
-
With
(CH3CO)2CH2;
In
water;
dissolving of powdered KMnO4 in water by slight warming, filtration, addn. of excess of distilled acetylacetone with vigorous stirring, stirring for 5 min over a steam-bath, allowing to cool for 10 min; filtration, washing several times with acetylacetone-water, vac. drying, recrystn. (benzene then light petroleum addn.), cooling to 0°C,elem. anal.;
DOI:10.1039/DT9820000669