(Zn(S₂P(OC₆H₄Me-p)2)2)

Base Information

• Chemical Name: (Zn(S₂P(OC₆H₄Me-p)2)2)
• CAS No.: 74895-05-9
• Molecular Formula: C₂₈H₂₈O₄P₂S₄Zn
• Molecular Weight: 684.129
• Mol file: 74895-05-9.mol

Synonyms:(Zn(S₂P(OC₆H₄Me-p)2)2)

Chemical Property of (Zn(S₂P(OC₆H₄Me-p)2)2)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Zn(S₂P(OC₆H₄Me-p)2)2)

There total 1 articles about (Zn(S₂P(OC₆H₄Me-p)2)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

zinc(II) sulfate heptahydrate + O,O-di-p-tolyl hydrogen phosphorodithioate (14366-43-9) → (Zn(S2P(OC6H4Me-p)2)2) (74895-05-9)

Guidance literature:

In water; toluene; to soln. HS2P(OC6H4Me-p)2 in toluene at room temp. added aq. soln. ZnSO4*7H2O and mixt. stirred overnight; organic layer separated, washed with water and evaporated in vacuo, oildissolved in diethyl ether-ligroin (b.p. 30-40°C) mixt. (1:1), soln. allowed to stand for 24 h, crystals filtered and washed with ligroin (b.p. 30-40°C); elem. anal.;

DOI:10.1039/DT9830000627

Reference yield: 45.0%

(Zn(S2P(OC6H4Me-p)2)2) (74895-05-9) + (NEt4)(S2CNMe2) → (NEt4)(Zn(S2P(OC6H4Me-p)2)2(S2CNMe2))*2H2O

Guidance literature:

In isopropyl alcohol; to soln. (Zn(S2P(OC6H4Me-p)2)2) in propan-2-ol added slowly with stirring soln. (NEt4)(S2CNMe2) in the same solvent; complex filtered; elem. anal.;

DOI:10.1039/DT9830000627

Reference yield: 40.0%

(Zn(S2P(OC6H4Me-p)2)2) (74895-05-9) + (NMe4)(S2P(OC6H4Me-p)2) → tetramethylammonium bis(OO'-di-p-tolyl dithiophosphato-S) (OO'-di-p-tolyl dithiophosphato-SS')zincate (77451-12-8)

Guidance literature:

In isopropyl alcohol; to soln. (Zn(S2P(OC6H4Me-p)2)2) in propan-2-ol added slowly with stirring and gentle heating suspn. (NMe4)(S2P(OC6H4Me-p)2) in propan-2-ol; soln. cooled, crystals filtered off and recrystd. from toluene; elem. anal.;

DOI:10.1039/DT9830000627

upstream raw materials:

O,O-di-p-tolyl hydrogen phosphorodithioate

Downstream raw materials:

tetramethylammonium bis(OO'-di-p-tolyl dithiophosphato-S) (OO'-di-p-tolyl dithiophosphato-SS')zincate

zinc stearate

(-S₂P(OC₆H₄Me-p)2)2

zinc(II) sulfate

Refernces