Technology Process of Karanjin
There total 13 articles about Karanjin which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 6 steps
1.1: K2CO3 / acetone / 6 h / Heating
2.1: 1.3 g / 2 h / 210 - 215 °C
3.1: OsO4; KIO4 / ethyl acetate; H2O
3.2: 230 mg / H3PO4 / 0.33 h / Heating
4.1: 70 mg / KOH / ethanol / 75 h / 20 °C
5.1: 0.51 g / 30 percent aq. H2O2; aq. NaOH; pyridine / 60 - 70 °C
6.1: 0.68 g / K2CO3 / acetone / 2 h / Heating
With
pyridine; potassium hydroxide; sodium hydroxide; osmium(VIII) oxide; potassium metaperiodate; dihydrogen peroxide; potassium carbonate;
In
ethanol; water; ethyl acetate; acetone;
2.1: Claisen rearrangement;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: OsO4; KIO4 / ethyl acetate; H2O
1.2: 230 mg / H3PO4 / 0.33 h / Heating
2.1: 70 mg / KOH / ethanol / 75 h / 20 °C
3.1: 0.51 g / 30 percent aq. H2O2; aq. NaOH; pyridine / 60 - 70 °C
4.1: 0.68 g / K2CO3 / acetone / 2 h / Heating
With
pyridine; potassium hydroxide; sodium hydroxide; osmium(VIII) oxide; potassium metaperiodate; dihydrogen peroxide; potassium carbonate;
In
ethanol; water; ethyl acetate; acetone;