Technology Process of 1-Phenylsilacyclohexane
There total 3 articles about 1-Phenylsilacyclohexane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
diethyl ether;
at 0 ℃;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/om4005725
- Guidance literature:
-
1‐phenyl‐1‐chloro‐1‐silacyclohexane;
With
lithium aluminium tetrahydride;
In
diethyl ether;
for 3h;
Reflux;
With
ammonium chloride;
In
diethyl ether; water; pentane;
at 20 ℃;
Saturated solution;
DOI:10.1016/j.tet.2011.10.082
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: magnesium
1.2: 6 h / Reflux
2.1: lithium aluminium tetrahydride / diethyl ether / 3 h / Reflux
2.2: 20 °C / Saturated solution
With
lithium aluminium tetrahydride; magnesium;
In
diethyl ether;
DOI:10.1016/j.tet.2011.10.082
