Methanesulfonamide, N-[2-[(4-amino-3-methylphenyl)ethylamino]ethyl]-

Base Information

• Chemical Name: Methanesulfonamide, N-[2-[(4-amino-3-methylphenyl)ethylamino]ethyl]-
• CAS No.: 92-09-1
• Deprecated CAS: 112207-63-3
• Molecular Formula: C12H21 N3 O2 S
• Molecular Weight: 271.384
• European Community (EC) Number: 202-124-2
• NSC Number: 517164
• UNII: 6VOV6V71VO
• DSSTox Substance ID: DTXSID4043779
• Nikkaji Number: J38.242F
• Wikidata: Q27265600
• ChEMBL ID: CHEMBL580441
• Mol file: 92-09-1.mol

Synonyms:CD 3 color developer;CD 3 color developer, phosphate (1:1);CD 3 color developer, sulfate (2:3);CD 3 color developer, sulfate, dihydrate (2:3);CD 3 color developer, sulfate, hydrate (2:3:1);CD-3 color developer;CD-3 Kodak

Chemical Property of Methanesulfonamide, N-[2-[(4-amino-3-methylphenyl)ethylamino]ethyl]-

Chemical Property:

• Vapor Pressure: 1.82E-08mmHg at 25°C
• Boiling Point: 455°C at 760 mmHg
• Flash Point: 229°C
• PSA: 83.81000
• Density: 1.204g/cm³
• LogP: 3.00560
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 6
• Exact Mass: 271.13544809
• Heavy Atom Count: 18
• Complexity: 340

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Chemical Classes: Nitrogen Compounds -> Amines, Aromatic
• Canonical SMILES: CCN(CCNS(=O)(=O)C)C1=CC(=C(C=C1)N)C

Technology Process of Methanesulfonamide, N-[2-[(4-amino-3-methylphenyl)ethylamino]ethyl]-

There total 3 articles about Methanesulfonamide, N-[2-[(4-amino-3-methylphenyl)ethylamino]ethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-chloroethyl)-methanesulfonamide (21896-59-3) + 4-(N-p-toluenesulfonyl)amino-3-methyl-N-ethylaniline (56891-62-4) → N-{2-[(4-amino-m-tolyl)ethylamino]ethyl}methanesulfonamide (92-09-1)

Guidance literature:

With sodium bicarbonate; sulfuric acid; In methanol; water;

Reference yield:

N-[2-(N-ethyl-3-methyl-4-nitroso-anilino)-ethyl]-methanesulfonamide (56046-62-9) → N-{2-[(4-amino-m-tolyl)ethylamino]ethyl}methanesulfonamide (92-09-1)

Guidance literature:

With ethanol; nickel; at 70 - 80 ℃; Hydrogenation;

DOI:10.1021/ja01151a037

Reference yield:

→ N-{2-[(4-amino-m-tolyl)ethylamino]ethyl}methanesulfonamide (92-09-1)

Guidance literature:

upstream raw materials:

N-[2-(N-ethyl-3-methyl-4-nitroso-anilino)-ethyl]-methanesulfonamide

N-(2-chloroethyl)-methanesulfonamide

4-(N-p-toluenesulfonyl)amino-3-methyl-N-ethylaniline

Downstream raw materials:

C₂₀H₂₇N₃O₃S

C₂₁H₂₈N₄O₄S

1,4-Naphtochinon-mono(4-amino>-2-methylphenylimin)

methyl-[1,4]benzoquinone-1-imine

Refernces

• 1、 -. "Transition metal complexes as dye forming catalysts in hair coloring compositions". . . Retrieved 2008/06/13.
• 2、 -. "Methine compounds". . . Retrieved 2008/06/13.