Technology Process of C15H12Cl2N6O4S2
There total 5 articles about C15H12Cl2N6O4S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
acetone;
at 0 ℃;
for 2h;
pH=6;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium carbonate / dimethyl sulfoxide / 1 h / 35 °C
1.2: 58 °C
2.1: dihydrogen peroxide / sodium tungstate (VI) dihydrate / water; acetic acid / 30 - 60 °C
3.1: trichlorophosphate / acetonitrile; ISOPROPYLAMIDE / 2 h / 45 - 60 °C
4.1: acetonitrile; water / 2.83 h / 5 °C
5.1: sodium hydroxide / acetone / 2 h / 0 °C / pH 6
With
dihydrogen peroxide; lithium carbonate; sodium hydroxide; trichlorophosphate;
sodium tungstate (VI) dihydrate;
In
ISOPROPYLAMIDE; water; acetic acid; dimethyl sulfoxide; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dihydrogen peroxide / sodium tungstate (VI) dihydrate / water; acetic acid / 30 - 60 °C
2: trichlorophosphate / acetonitrile; ISOPROPYLAMIDE / 2 h / 45 - 60 °C
3: acetonitrile; water / 2.83 h / 5 °C
4: sodium hydroxide / acetone / 2 h / 0 °C / pH 6
With
dihydrogen peroxide; sodium hydroxide; trichlorophosphate;
sodium tungstate (VI) dihydrate;
In
ISOPROPYLAMIDE; water; acetic acid; acetone; acetonitrile;