2-nitro-benzenesulfenic acid-[1]naphthylamide

Base Information

• Chemical Name: 2-nitro-benzenesulfenic acid-[1]naphthylamide
• CAS No.: 78945-08-1
• Molecular Formula: C₁₆H₁₂N₂O₂S
• Molecular Weight: 296.349
• Mol file: 78945-08-1.mol

Synonyms:2-nitro-benzenesulfenic acid-[1]naphthylamide

Chemical Property of 2-nitro-benzenesulfenic acid-[1]naphthylamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-nitro-benzenesulfenic acid-[1]naphthylamide

There total 3 articles about 2-nitro-benzenesulfenic acid-[1]naphthylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

2-nitrobenzenesulfenyl bromide (22024-99-3) + 1-amino-naphthalene (134-32-7) → 2-nitro-benzenesulfenic acid-[1]naphthylamide (78945-08-1)

Guidance literature:

With triethylamine; In dichloromethane; at 18 - 20 ℃; for 24h;

Reference yield:

bis(2-nitrophenyl)disulfide (1155-00-6) → 2-nitro-benzenesulfenic acid-[1]naphthylamide (78945-08-1)

Guidance literature:

Multi-step reaction with 2 steps

1: CCl₄; chlorine / unter Ausschluss der Luftfeuchtigkeit

2: chloroform

With tetrachloromethane; chloroform; chlorine;

Reference yield:

2-Chloronitrobenzene (88-73-3) → 2-nitro-benzenesulfenic acid-[1]naphthylamide (78945-08-1)

Guidance literature:

Multi-step reaction with 3 steps

1: Na₂S₂

2: CCl₄; chlorine / unter Ausschluss der Luftfeuchtigkeit

3: chloroform

With tetrachloromethane; sodium disulfide; chloroform; chlorine;

upstream raw materials:

2-nitrobenzenesulfenyl bromide

1-amino-naphthalene

bis(2-nitrophenyl)disulfide

2-Chloronitrobenzene

Downstream raw materials:

2-nitrobenzenesulfenyl chloride

ethyl (naphthalen-1-yl)carbamate

N-1-naphthalenyl-benzamide

bis(2-nitrophenyl)disulfide

Refernces