Technology Process of Nitroscanate
There total 8 articles about Nitroscanate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
iron(II) sulfate; triethylamine;
In
acetone;
at 20 ℃;
for 2h;
chemoselective reaction;
DOI:10.1080/00397910802448481
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / N,N-dimethyl-formamide / 20 - 140 °C
2: hydrogenchloride; water / methanol / 0.33 h / Reflux
3: water / 2 h / 100 °C
4: pyridine / 5,5-dimethyl-1,3-cyclohexadiene / 0.75 h / 140 °C
With
pyridine; hydrogenchloride; water; potassium carbonate;
In
methanol; 5,5-dimethyl-1,3-cyclohexadiene; water; N,N-dimethyl-formamide;
DOI:10.1007/s11164-015-2123-1
