1-(trifluoromethyl)-2-chloroethyl phenyl selenide

Base Information

• Chemical Name: 1-(trifluoromethyl)-2-chloroethyl phenyl selenide
• CAS No.: 73194-30-6
• Molecular Formula: C₉H₈ClF₃Se
• Molecular Weight: 287.571
• Mol file: 73194-30-6.mol

Synonyms:1-(trifluoromethyl)-2-chloroethyl phenyl selenide

Chemical Property of 1-(trifluoromethyl)-2-chloroethyl phenyl selenide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1-(trifluoromethyl)-2-chloroethyl phenyl selenide

There total 1 articles about 1-(trifluoromethyl)-2-chloroethyl phenyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Phenylselenyl chloride (5707-04-0) + 1,1,1-trifluoropropylene (677-21-4) → 1-(trifluoromethyl)-2-chloroethyl phenyl selenide (73194-30-6)

Guidance literature:

In dichloromethane; 1) dry ice/acetone, 2) 60 deg C, overnight;

DOI:10.1021/jo01298a041

Reference yield: 95.0%

1-(trifluoromethyl)-2-chloroethyl phenyl selenide (73194-30-6) → 1-(trifluoromethyl)ethenyl phenyl selenide (73194-32-8)

Guidance literature:

With potassium hydroxide; In methanol; at 10 ℃; for 0.166667h;

DOI:10.1021/jo01298a041

Reference yield: 3.0%

methanol (67-56-1) + 1-(trifluoromethyl)-2-chloroethyl phenyl selenide (73194-30-6) → 1-(trifluoromethyl)ethenyl phenyl selenide (73194-32-8) + 2-methoxy-(trifluoromethyl)ethyl phenyl selenide (73194-34-0)

Guidance literature:

With potassium hydroxide; for 2h; Ambient temperature;

DOI:10.1021/jo01298a041

upstream raw materials:

Phenylselenyl chloride

1,1,1-trifluoropropylene

Downstream raw materials:

1-(trifluoromethyl)ethenyl phenyl selenide

2-methoxy-(trifluoromethyl)ethyl phenyl selenide

butyl phenyl selenide

6-Fluoro-2-methyl-5-phenylselanyl-4H-pyran-3-carboxylic acid ethyl ester

Refernces