3-methoxy-N,N-bis(3-methylbut-2-enyl)aniline hydrochloride

Base Information

• Chemical Name: 3-methoxy-N,N-bis(3-methylbut-2-enyl)aniline hydrochloride
• CAS No.: 1073190-52-9
• Molecular Formula: C₁₇H₂₅NO*ClH
• Molecular Weight: 295.853
• Mol file: 1073190-52-9.mol

Synonyms:3-methoxy-N,N-bis(3-methylbut-2-enyl)aniline hydrochloride

Chemical Property of 3-methoxy-N,N-bis(3-methylbut-2-enyl)aniline hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-methoxy-N,N-bis(3-methylbut-2-enyl)aniline hydrochloride

There total 1 articles about 3-methoxy-N,N-bis(3-methylbut-2-enyl)aniline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-methoxy-N,N-bis(3-methyl-2-buten-1-yl)benzenamine (1073190-51-8) → 3-methoxy-N,N-bis(3-methylbut-2-enyl)aniline hydrochloride (1073190-52-9)

Guidance literature:

With hydrogenchloride; In water; N,N-dimethyl-formamide; at 0 ℃;

DOI:10.1021/ol801904k

Reference yield: 52.0%

3-methoxy-N,N-bis(3-methylbut-2-enyl)aniline hydrochloride (1073190-52-9) → 1,1,7,7-tetramethyl-2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinolin-8-ol (115704-83-1)

Guidance literature:

3-methoxy-N,N-bis(3-methylbut-2-enyl)aniline hydrochloride; With methanesulfonic acid; at 95 ℃; for 24h;

With ammonium hydroxide; In water;

upstream raw materials:

3-methoxy-N,N-bis(3-methyl-2-buten-1-yl)benzenamine

Downstream raw materials:

1,1,7,7-tetramethyl-2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinolin-8-ol

Refernces

• 1、 Uddin, Md Jashim,Marnett, Lawrence J.. "Synthesis of 5- and 6-carboxy-x-rhodamines". supporting information; experimental part. p. 4799 - 4801. Retrieved 2009/05/31.