2,4-dibromophenyl dimethylcarbamate

Base Information

• Chemical Name: 2,4-dibromophenyl dimethylcarbamate
• CAS No.: 1380586-39-9
• Molecular Formula: C₉H₉Br₂NO₂
• Molecular Weight: 322.984
• Mol file: 1380586-39-9.mol

Synonyms:2,4-dibromophenyl dimethylcarbamate

Chemical Property of 2,4-dibromophenyl dimethylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 2,4-dibromophenyl dimethylcarbamate

There total 2 articles about 2,4-dibromophenyl dimethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

4-bromophenyl dimethylcarbamate (7308-55-6) → 2,4-dibromophenyl dimethylcarbamate (1380586-39-9)

Guidance literature:

With N-Bromosuccinimide; palladium diacetate; toluene-4-sulfonic acid; In 1,2-dichloro-ethane; at 60 - 90 ℃; for 16h; Inert atmosphere;

DOI:10.1021/jo300713h

Reference yield:

4-bromo-phenol (106-41-2) → 2,4-dibromophenyl dimethylcarbamate (1380586-39-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 5 h / Inert atmosphere; Reflux

2: N-Bromosuccinimide; palladium diacetate; toluene-4-sulfonic acid / 1,2-dichloro-ethane / 16 h / 60 - 90 °C / Inert atmosphere

With N-Bromosuccinimide; palladium diacetate; potassium carbonate; toluene-4-sulfonic acid; In 1,2-dichloro-ethane; acetonitrile;

DOI:10.1021/jo300713h

upstream raw materials:

4-bromo-phenol

4-bromophenyl dimethylcarbamate

Refernces