N,N-diethyl-4-((4-nitrophenyl)diazenyl)aniline

Base Information

• Chemical Name: N,N-diethyl-4-((4-nitrophenyl)diazenyl)aniline
• CAS No.: 80631-73-8
• Molecular Formula: C₁₆H₁₈N₄O₂
• Molecular Weight: 298.345
• Mol file: 80631-73-8.mol

Synonyms:N,N-diethyl-4-((4-nitrophenyl)diazenyl)aniline

Chemical Property of N,N-diethyl-4-((4-nitrophenyl)diazenyl)aniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-diethyl-4-((4-nitrophenyl)diazenyl)aniline

There total 2 articles about N,N-diethyl-4-((4-nitrophenyl)diazenyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-diethylamino-4'-nitroazobenzene (80631-72-7) → N,N-diethyl-4-((4-nitrophenyl)diazenyl)aniline (80631-73-8)

Guidance literature:

With sodium bis(2-ethylhexyl)-sulfosuccinate; In n-heptane; water; Equilibrium constant; Rate constant; Irradiation; further solvents, further conditions;

DOI:10.1021/ja00360a043

Reference yield:

4-nitro-aniline (100-01-6,104810-17-5) + N,N-diethylaniline (91-66-7) → N,N-diethyl-4-((4-nitrophenyl)diazenyl)aniline (80631-73-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium nitrite; hydrogenchloride / water; acetone / 0.5 h / 5 °C

1.2: 2 h / 5 °C

2.1: tetrahydrofuran / Irradiation

With hydrogenchloride; sodium nitrite; In tetrahydrofuran; water; acetone;

DOI:10.1039/c4tc00996g

Reference yield:

N,N-diethyl-4-((4-nitrophenyl)diazenyl)aniline (80631-73-8) → 4-diethylamino-4'-nitroazobenzene (80631-72-7)

Guidance literature:

In n-heptane; at 25 ℃; Rate constant; Thermodynamic data; Kinetics; var. solvents; var. temp.; ΔG_ct. (excit), E_max , ΔH_ct. (excit), ΔS_ct (excit), mechanism;

DOI:10.1021/jo00165a005

upstream raw materials:

4-diethylamino-4'-nitroazobenzene

4-nitro-aniline

N,N-diethylaniline

Downstream raw materials:

4-diethylamino-4'-nitroazobenzene

Refernces

• 1、 Schanze, Kirk S.,Whitten, David G.. "Solubilization in Surfactant Media: Use of an Isomerizable Solute Probe To Determine Microheterogeneity in Microemulsions". . p. 6734 - 6735. Retrieved 2007/10/02.