HIPPURIC ACID SODIUM SALT

Base Information

• Chemical Name: HIPPURIC ACID SODIUM SALT
• CAS No.: 532-94-5
• Molecular Formula: C9H9 N O3 . Na
• Molecular Weight: 201.157
• Hs Code.: 2924299090
• Mol file: 532-94-5.mol

Synonyms:Glycine,N-benzoyl-, monosodium salt (9CI); Hippuric acid, monosodium salt (8CI);Hippuric acid sodium salt; N-Benzoylglycine sodium salt; Sodium hippurate

Chemical Property of HIPPURIC ACID SODIUM SALT

Chemical Property:

• Appearance/Colour: white to off-white powder
• Vapor Pressure: 2.06E-09mmHg at 25°C
• Melting Point: 240～244℃
• Boiling Point: 464.1 °C at 760 mmHg
• Flash Point: 234.5 °C
• PSA: 69.23000
• Density: g/cm³
• LogP: -0.44280
• Storage Temp.: Store at RT.
• Solubility.: H2O: 0.5 M at 20 °C, clear, colorless
• Water Solubility.: Soluble in water.

Purity/Quality:

98%,99%, ^*data from raw suppliers

Hippuric acid sodium salt 99+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22-36/37/38
• Safety Statements: 24/25-36/37-26-22

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Uses: Hippuric Acid Sodium Salt can be used for agrobacterium-mediated rice genetic transformation method.

Technology Process of HIPPURIC ACID SODIUM SALT

There total 1 articles about HIPPURIC ACID SODIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoyl chloride (98-88-4) + glycine (56-40-6,18875-39-3,25718-94-9) → sodium hippurate (532-94-5)

Guidance literature:

With sodium hydroxide;

DOI:10.1080/00397911.2017.1340649

Reference yield: 99.0%

sodium hippurate (532-94-5) + benzaldehyde (100-52-7) → 4-benzylidene-2-phenyloxazole-5(4H)-one (842-74-0,5839-91-8)

Guidance literature:

With sodium acetate; acetic anhydride; triethylamine sulfate; In neat (no solvent); at 90 ℃; Solvent; Temperature; Green chemistry;

DOI:10.1080/00397911.2017.1340649

Reference yield: 98.0%

sodium hippurate (532-94-5) + 4-methoxy-benzaldehyde (123-11-5) → 4-(4-methoxybenzylidene)-2-phenyl-5(4H)-oxazolone (5429-22-1)

Guidance literature:

With sodium acetate; acetic anhydride; triethylamine sulfate; In neat (no solvent); at 90 ℃; Green chemistry;

DOI:10.1080/00397911.2017.1340649

upstream raw materials:

benzoyl chloride

glycine

Downstream raw materials:

2-phenyl-4-butyryl-5-oxazolinone

(Z)-2-phenyl-4-piperonylidene-2-oxazoline-5(4H)-one

2-phenyl-4-acetyl-5-oxazolinone

2-phenyl-4-propionyl-5-oxazolinone

Refernces