nickel⁽⁰⁾ 1,10-phenanthroline complex

Base Information

• Chemical Name: nickel⁽⁰⁾ 1,10-phenanthroline complex
• CAS No.: 10170-11-3
• Molecular Formula: C₂₄H₁₆N₄Ni
• Molecular Weight: 419.108
• Mol file: 10170-11-3.mol

Synonyms:nickel⁽⁰⁾ 1,10-phenanthroline complex

Chemical Property of nickel⁽⁰⁾ 1,10-phenanthroline complex

Chemical Property:

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Technology Process of nickel⁽⁰⁾ 1,10-phenanthroline complex

There total 1 articles about nickel⁽⁰⁾ 1,10-phenanthroline complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,10-Phenanthroline (66-71-7) + {methyl(trimethylphosphine)4}nickel(II) tetrafluoroborate → nickel(0) 1,10-phenanthroline complex (10170-11-3) + tetramethylphosphonium (32589-80-3) + trimethylphosphane (594-09-2)

Guidance literature:

In methanol; addn. of excess of ligand to a soln. of the complex in methanol, warming to 50°C for 45 min; removal of volatiles, extn. of residue with light petroleum, filtn., concg. of filtrate, standing at -15°C;

upstream raw materials:

1,10-Phenanthroline