resveratrol trimethacrylate

Base Information

• Chemical Name: resveratrol trimethacrylate
• CAS No.: 1236211-47-4
• Molecular Formula: C₂₆H₂₄O₆
• Molecular Weight: 432.473
• Mol file: 1236211-47-4.mol

Synonyms:resveratrol trimethacrylate

Chemical Property of resveratrol trimethacrylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of resveratrol trimethacrylate

There total 7 articles about resveratrol trimethacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-5-[2-4-(hydroxyphenyl)ethenyl]-1,3-benzenediol (501-36-0) + Methacryloyl chloride (920-46-7,26937-45-1) → resveratrol trimethacrylate (1236211-47-4)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at 0 - 20 ℃; for 48h;

Reference yield:

(E)-5-[2-4-(hydroxyphenyl)ethenyl]-1,3-benzenediol (501-36-0) + sodium sulfate (7757-82-6) + Methacryloyl chloride (920-46-7,26937-45-1) → resveratrol trimethacrylate (1236211-47-4)

Guidance literature:

In ice-water; hexane; ethyl acetate; triethylamine; acetonitrile;

Reference yield:

3,5-diacetoxybenzoic acid (35354-29-1) → resveratrol trimethacrylate (1236211-47-4)

Guidance literature:

Multi-step reaction with 3 steps

1: thionyl chloride; N-ethylmorpholine; / palladium diacetate / ethyl acetate; N,N-dimethyl-formamide; toluene

2: potassium hydroxide / ethyl acetate; methanol

3: ethyl acetate; triethylamine; hexane; acetonitrile; ice-water

With N-ethylmorpholine;; potassium hydroxide; thionyl chloride; palladium diacetate; In methanol; ice-water; hexane; ethyl acetate; triethylamine; N,N-dimethyl-formamide; toluene; acetonitrile;

upstream raw materials:

3,5-diacetoxybenzoic acid

p-acetoxystyrene

3,5-diacetoxybenzoyl chloride

(E)-5-[2-4-(hydroxyphenyl)ethenyl]-1,3-benzenediol

Refernces