C₁₂H₁₆BrNO₃S

Base Information

• Chemical Name: C₁₂H₁₆BrNO₃S
• CAS No.: 1197341-37-9
• Molecular Formula: C₁₂H₁₆BrNO₃S
• Molecular Weight: 334.234
• Mol file: 1197341-37-9.mol

Synonyms:C₁₂H₁₆BrNO₃S

Chemical Property of C₁₂H₁₆BrNO₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₂H₁₆BrNO₃S

There total 1 articles about C₁₂H₁₆BrNO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-bromoacetyl chloride (22118-09-8) + N-butylbenzenesulfonamide (3622-84-2) → C12H16BrNO3S (1197341-37-9)

Guidance literature:

N-butylbenzenesulfonamide; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.583333h; Inert atmosphere;

2-bromoacetyl chloride; In tetrahydrofuran; at -78 - 20 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tetlet.2009.08.125

Reference yield:

C12H16BrNO3S (1197341-37-9) → C12H17NO3S (1197341-39-1) + N-butylbenzenesulfonamide (3622-84-2)

Guidance literature:

With dichloromethane; N,N,N',N'',N'''-pentamethyldiethylenetriamine; copper(I) bromide; for 4h; Reflux; Inert atmosphere;

DOI:10.1016/j.tetlet.2009.08.125

upstream raw materials:

2-bromoacetyl chloride

N-butylbenzenesulfonamide

Downstream raw materials:

C₁₂H₁₇NO₃S

N-butylbenzenesulfonamide

Refernces