Technology Process of C24H32O10S5
There total 5 articles about C24H32O10S5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate;
In
dichloromethane;
at 20 ℃;
for 18h;
Inert atmosphere;
DOI:10.1039/c3cc49704f
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine; dmap / dichloromethane / 18 h / 20 °C / Inert atmosphere
2: 10 wt% Pd(OH)2 on carbon; hydrogen / dichloromethane; methanol / 16 h / 20 °C / 7500.75 Torr
3: 4-(dimethylamino)pyridinium tosylate; dicyclohexyl-carbodiimide / dichloromethane / 18 h / 20 °C / Inert atmosphere
With
pyridine; dmap; 10 wt% Pd(OH)2 on carbon; hydrogen; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate;
In
methanol; dichloromethane;
DOI:10.1039/c3cc49704f
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 10 wt% Pd(OH)2 on carbon; hydrogen / dichloromethane; methanol / 16 h / 20 °C / 7500.75 Torr
2: 4-(dimethylamino)pyridinium tosylate; dicyclohexyl-carbodiimide / dichloromethane / 18 h / 20 °C / Inert atmosphere
With
10 wt% Pd(OH)2 on carbon; hydrogen; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate;
In
methanol; dichloromethane;
DOI:10.1039/c3cc49704f