Technology Process of m-nitrophenyl salicylate
There total 3 articles about m-nitrophenyl salicylate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dipotassium hydrogenphosphate; 9-(2-mesityl)-10-methylacridinium perchlorate;
In
acetonitrile;
at 40 ℃;
for 26h;
Irradiation;
Inert atmosphere;
DOI:10.1002/anie.201706597
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 10 h / 100 °C / Inert atmosphere
2: potassium permanganate / water / 10 h / 85 °C
3: 9-(2-mesityl)-10-methylacridinium perchlorate; dipotassium hydrogenphosphate / acetonitrile / 26 h / 40 °C / Irradiation; Inert atmosphere
With
potassium permanganate; dipotassium hydrogenphosphate; potassium carbonate; 9-(2-mesityl)-10-methylacridinium perchlorate;
In
water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/anie.201706597
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 10 h / 100 °C / Inert atmosphere
2: potassium permanganate / water / 10 h / 85 °C
3: 9-(2-mesityl)-10-methylacridinium perchlorate; dipotassium hydrogenphosphate / acetonitrile / 26 h / 40 °C / Irradiation; Inert atmosphere
With
potassium permanganate; dipotassium hydrogenphosphate; potassium carbonate; 9-(2-mesityl)-10-methylacridinium perchlorate;
In
water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/anie.201706597
