Technology Process of benzyl 4,6-O-benzylidene-α-D-glucopyranoside
There total 5 articles about benzyl 4,6-O-benzylidene-α-D-glucopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid; triethylamine;
In
N,N-dimethyl-formamide;
at 40 - 45 ℃;
for 2h;
Yield given;
DOI:10.1016/S0008-6215(82)80007-4
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) AcCl; 2.) Amberlist 21 (OH-) / 1.) 3 days at 15-20 deg C, 1 day at 50 deg C
2: 1.) TsOH*H2O; 2.) Et3N / dimethylformamide / 2 h / 40 - 45 °C
With
Amberlist 21 (OH-); toluene-4-sulfonic acid; triethylamine; acetyl chloride;
In
N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(82)80007-4
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) AcCl; 2.) Amberlist 21 (OH-) / 1.) 3 days at 15-20 deg C, 1 day at 50 deg C
2: 1.) TsOH*H2O; 2.) Et3N / dimethylformamide / 2 h / 40 - 45 °C
With
Amberlist 21 (OH-); toluene-4-sulfonic acid; triethylamine; acetyl chloride;
In
N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(82)80007-4
