3-ureidomethyl-3,5,5-trimethylcyclohexyl urea

Base Information

• Chemical Name: 3-ureidomethyl-3,5,5-trimethylcyclohexyl urea
• CAS No.: 78632-23-2
• Molecular Formula: C₁₂H₂₄N₄O₂
• Molecular Weight: 256.348
• Mol file: 78632-23-2.mol

Synonyms:3-ureidomethyl-3,5,5-trimethylcyclohexyl urea

Chemical Property of 3-ureidomethyl-3,5,5-trimethylcyclohexyl urea

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-ureidomethyl-3,5,5-trimethylcyclohexyl urea

There total 3 articles about 3-ureidomethyl-3,5,5-trimethylcyclohexyl urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-aminomethyl-3,5,5-trimethylcyclohexylamine + urea (57-13-6) → 3-ureidomethyl-3,5,5-trimethylcyclohexyl urea (78632-23-2)

Guidance literature:

With phenol; at 50 - 120 ℃; for 3.5h; Reagent/catalyst; Temperature; Inert atmosphere;

Reference yield: 98.0%

3-aminomethyl-3,5,5-trimethylcyclohexylamine (2855-13-2) + urea (57-13-6) → 3-ureidomethyl-3,5,5-trimethylcyclohexyl urea (78632-23-2)

Guidance literature:

In water; at 90 - 220 ℃; under 9750.98 Torr; Industry scale;

Reference yield: 93.7%

→ 3-ureidomethyl-3,5,5-trimethylcyclohexyl urea (78632-23-2)

Guidance literature:

With N-benzyl-trimethylammonium hydroxide; In 2-methoxy-ethanol; at 100 ℃; for 3h;

upstream raw materials:

3-aminomethyl-3,5,5-trimethylcyclohexylamine

urea

Downstream raw materials:

3-((4-(α,α-dimethylbenzyl)phenoxy)carbonylaminomethyl)-3,5,5-trimethylcyclohexyl carbamic acid (4-(α,α-dimethylbenzyl)phenyl)ester

3-((p-dodecylphenyloxy)carbonylamidomethyl)-3,5,5-trimethylcyclohexyl carbamic acid (p-dodecylphenyl) ester

3-((4-tert-amylphenoxy)carbonylamino-methyl)-3,5,5-trimethylcyclohexyl carbamic acid (4-tert-amylphenyl) ester

3-((4-(1,1,3,3-tetramethylbutyl)phenoxy)carbonylamino-methyl)-3,5,5-trimethylcyclohexyl carbamic acid (4-(1,1,3,3-tetramethylbutyl)phenyl) ester

Refernces

• 1、 -. "Method for Preparing Diureido Compounds". Paragraph 0037; 0056-0058. . Retrieved 2016/12/22.
• 2、 -. "PROCESS FOR THE PREPARATION OF N-SUBSTITUTED CARBAMIC ACID ESTER AND PROCESS FOR THE PREPARATION OF ISOCYANATE USING THE N-SUBSTITUTED CARBAMIC ACID ESTER". Page/Page column 128. . Retrieved 2011/06/10.