N-(2-Methoxyphenyl)-3-phenylpropenamide

Base Information Edit

Chemical Name:N-(2-Methoxyphenyl)-3-phenylpropenamide
CAS No.:6889-84-5
Molecular Formula:C₁₆H₁₅NO₂
Molecular Weight:253.301
Hs Code.:
Mol file:6889-84-5.mol

Synonyms:N-(2-methoxyphenyl)-3-phenylacrylamide

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Chemical Property of N-(2-Methoxyphenyl)-3-phenylpropenamide Edit

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Technology Process of N-(2-Methoxyphenyl)-3-phenylpropenamide

There total 6 articles about N-(2-Methoxyphenyl)-3-phenylpropenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.3%

: 102-92-1,17082-09-6
cinnamoyl chloride

: 90-04-0
2-methoxy-phenylamine

: 6889-84-5
N-(2-methoxyphenyl)-3-phenylacrylamide

Guidance literature:: With dmap; In dichloromethane; at 0 - 30 ℃;

Reference yield: 87.0%

: 90-04-0
2-methoxy-phenylamine

: 621-82-9
Cinnamic acid

: 6889-84-5
N-(2-methoxyphenyl)-3-phenylacrylamide

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; for 6h;
DOI:10.1016/j.bmcl.2013.01.027

Reference yield: 48.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 91-23-6
2-Nitroanisole

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 6889-84-5
N-(2-methoxyphenyl)-3-phenylacrylamide

Guidance literature:: With bis(acetylacetonato)palladium(II); 1,3-bis-(diphenylphosphino)propane; benzenesulfonic acid; In 1,4-dioxane; at 130 ℃; for 14h; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.8b02109