Azoxybenzene-4,4'-disulphonamide

Base Information

• Chemical Name: Azoxybenzene-4,4'-disulphonamide
• CAS No.: 5187-79-1
• Molecular Formula: C₁₂H₁₂N₄O₅S₂
• Molecular Weight: 356.383
• Mol file: 5187-79-1.mol

Synonyms:Azoxybenzene-4,4'-disulphonamide

Chemical Property of Azoxybenzene-4,4'-disulphonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Azoxybenzene-4,4'-disulphonamide

There total 13 articles about Azoxybenzene-4,4'-disulphonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sulphaacetamide (144-80-9) → sulfanilamide (63-74-1) + Azobenzene-4,4'-disulphonamide (4320-29-0) + 4,4'-azo-bis-benzenesulfonic acid (2779-21-7) + Azoxybenzene-4,4'-disulphonamide (5187-79-1)

Guidance literature:

With 0.01percent antioxidant or without; In water; at 28 ℃; for 2h; Further byproducts given; Irradiation;

Reference yield:

sulphaacetamide (144-80-9) → Azoxybenzene-4,4'-disulphonic acid (83796-87-6) + sulfanilamide (63-74-1) + Azobenzene-4,4'-disulphonamide (4320-29-0) + 4,4'-azo-bis-benzenesulfonic acid (2779-21-7) + 4-aminobenzene sulfonic acid (121-57-3,856062-06-1) + Azoxybenzene-4,4'-disulphonamide (5187-79-1)

Guidance literature:

With antioxidant; In water; at 28 ℃; for 2h; Product distribution; Irradiation; without antioxidant, λ max 254 nm;

Reference yield:

4-(hydroxyamino) benzene sulfonamide (877-67-8) + water (7732-18-5) → sulfanilamide (63-74-1) + Azoxybenzene-4,4'-disulphonamide (5187-79-1)

Guidance literature:

at 23 ℃; Kinetics; sowie bei 37grad und 39grad; pH 7.3.Hydrolysis;

upstream raw materials:

sulfanilamide

4-nitro-N-(1,3,3-trimethyl-1,3-dihydro-indol-2-ylidene)-benzenesulfonamide

sulphaacetamide

dihydrogen peroxide

Downstream raw materials:

hydrazobenzene-4,4'-disulfonamide

sulfanilamide

Refernces

• 1、 Srivastava, S. P.,Mittal, A. K.,Gupta, V. K.. "Kinetics and Mechanism of Oxidation of Sulphanilamide, Sodium Sulphacetamide, Sulphasomidine, Sulphaguanidine, Sulphadiazine, Sulphapyridine and Sulphamethiazole by Peroxydisulphate Ion". . p. 806 - 809. Retrieved 2007/10/02.