2-Butoxynaphthalene

Base Information

• Chemical Name: 2-Butoxynaphthalene
• CAS No.: 10484-56-7
• Molecular Formula: C14H16 O
• Molecular Weight: 200.28
• European Community (EC) Number: 233-998-3
• UNII: I8O56IV62A
• DSSTox Substance ID: DTXSID7065093
• Nikkaji Number: J117.457F
• Wikidata: Q27280580
• Mol file: 10484-56-7.mol

Synonyms:2-Butoxynaphthalene;10484-56-7;Naphthalene, 2-butoxy-;Butyl beta-naphthyl ether;Butyl 2-naphthyl ether;UNII-I8O56IV62A;I8O56IV62A;EINECS 233-998-3;AI3-20476;2-n-butoxynaphthalene;2-Butoxynaphthalene #;beta-Naphthol butyl ether;.beta.-Naphthol butyl ether;SCHEMBL470925;DTXSID7065093;FEMA NO. 4634;AMY7772;.BATA.-NAPHTHOL BUTYL ETHER;BCP22243;BUTYL .BETA.-NAPHTHYL ETHER;MFCD00068798;AKOS016011258;DS-6573;2-butoxynaphthalene, butyl naphthyl ether;CS-0078406;FT-0636712;D71124;Q27280580

Chemical Property of 2-Butoxynaphthalene

Chemical Property:

• Vapor Pressure: 0.000817mmHg at 25°C
• Melting Point: 35-36℃
• Boiling Point: 315.3°Cat760mmHg
• Flash Point: 123.5°C
• PSA: 9.23000
• Density: 1.016g/cm³
• LogP: 4.01870
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: Acetonitrile (Slightly), Chloroform (Slightly)
• XLogP3: 4.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 200.120115130
• Heavy Atom Count: 15
• Complexity: 178

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-Butoxynaphthalene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCOC1=CC2=CC=CC=C2C=C1

Technology Process of 2-Butoxynaphthalene

There total 14 articles about 2-Butoxynaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-bromo-butane (109-65-9) + β-naphthol (135-19-3) → 2-butoxynaphthalene (10484-56-7)

Guidance literature:

With potassium hydroxide; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; Ambient temperature;

DOI:10.1039/a806328a

Reference yield: 98.0%

2-Methoxynaphthalene (93-04-9) + butan-1-ol (71-36-3) → 2-butoxynaphthalene (10484-56-7)

Guidance literature:

With bismuth(lll) trifluoromethanesulfonate; In water; 1,2-dichloro-ethane; at 110 ℃; for 24h; Schlenk technique; Inert atmosphere;

DOI:10.1246/cl.180361

Reference yield: 97.0%

β-naphthol (135-19-3) + butan-1-ol (71-36-3) → 2-butoxynaphthalene (10484-56-7)

Guidance literature:

With Nafion NR₅₀; at 115 ℃; for 35h; Inert atmosphere; Large scale reaction;

DOI:10.1039/c1gc15481h

upstream raw materials:

1-bromo-butane

potassium 2-naphthoxide

sodium 2-naphtholate

butyl para-toluenesulfonate

Downstream raw materials:

2-Methylnaphthalene

2,2'-binaphthalene

2-phenylnaphthalene

C_.I_. pigment orange 5

Refernces

• 1、 Bradshaw et al.. "-". . p. 259. Retrieved 1968.
• 2、 Murai, Masahito,Origuchi, Kazuki,Takai, Kazuhiko. "Catalytic cleavage and reformation of ethereal σ-bonds". . p. 927 - 930. Retrieved 2018.
• 3、 Balint, Erika,Kovacs, Orsolya,Drahos, Laszlo,Keglevich, Gyoergy. "Microwave-Assisted solid-liquid phase alkylation of naphthols". . p. 330 - 336. Retrieved 2013/07/26.