4,4'-e,e-cyclohexylcyclohexanediol

Base Information

• Chemical Name: 4,4'-e,e-cyclohexylcyclohexanediol
• CAS No.: 46310-14-9
• Molecular Formula: C₁₂H₂₂O₂
• Molecular Weight: 198.305
• Mol file: 46310-14-9.mol

Synonyms:4,4'-e,e-cyclohexylcyclohexanediol

Chemical Property of 4,4'-e,e-cyclohexylcyclohexanediol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4'-e,e-cyclohexylcyclohexanediol

There total 9 articles about 4,4'-e,e-cyclohexylcyclohexanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4'-Dihydroxybiphenyl (92-88-6) → 4,4'-a,e-cyclohexylcyclohexanediol (20601-38-1,46310-12-7,46310-13-8,46310-14-9)

Guidance literature:

With ethanol; nickel; at 150 - 200 ℃; under 110326 - 183877 Torr; Hydrogenation;

DOI:10.1021/ja01337a060 DOI:10.1021/ja01188a518 DOI:10.1021/ja01177a539

Reference yield:

cyclohexylcyclohexane (92-51-3) → 4,4'-e,e-cyclohexylcyclohexanediol (46310-14-9) + 4,4'-a,e-cyclohexylcyclohexanediol (20601-38-1,46310-12-7,46310-13-8,46310-14-9) + 3,4'-e,e-cyclohexylcyclohexanediol (102518-57-0)

Guidance literature:

Gongronella lacrispora; In N,N-dimethyl-formamide; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(86)80056-9

Reference yield:

cyclohexylcyclohexane (92-51-3) → 4,4'-e,e-cyclohexylcyclohexanediol (46310-14-9) + 4,4'-a,e-cyclohexylcyclohexanediol (20601-38-1,46310-12-7,46310-13-8,46310-14-9) + 3,4'-e,e-cyclohexylcyclohexanediol (102518-57-0)

Guidance literature:

Gongronella lacrispora; In N,N-dimethyl-formamide; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(86)80056-9

upstream raw materials:

cyclohexylcyclohexane

ethanol

4,4'-Dihydroxybiphenyl

Downstream raw materials:

C₃₈H₅₄O₈

trans,trans-4,4'-bicyclohexyl-bis{4-[6-(benzyloxy)hexan-1-oxy]benzoate}

4'-hydroxycyclohexylcyclohexan-4-one

4,4'-bicyclohexanone

Refernces