bicyclo{2.2.1}hept-1-yltrimethylstannane

Base Information

• Chemical Name: bicyclo{2.2.1}hept-1-yltrimethylstannane
• CAS No.: 42204-95-5
• Molecular Formula: C₁₀H₂₀Sn
• Molecular Weight: 258.979
• Mol file: 42204-95-5.mol

Synonyms:bicyclo{2.2.1}hept-1-yltrimethylstannane

Chemical Property of bicyclo{2.2.1}hept-1-yltrimethylstannane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of bicyclo{2.2.1}hept-1-yltrimethylstannane

There total 2 articles about bicyclo{2.2.1}hept-1-yltrimethylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1-iodonorbornane (930-80-3) + trimethylstannyl sodium (16643-09-7) → norbornene (279-23-2) + bicyclo{2.2.1}hept-1-yltrimethylstannane (42204-95-5)

Guidance literature:

With dicyclohexylphosphane; In tetrahydrofuran; at 0 ℃; for 0.0833333h; Product distribution; Mechanism; other trapping agents or none, other solvent, other time;

DOI:10.1021/jo00085a012

Reference yield: 12.0%

1-bromonorbornane (13474-70-9) + trimethylstannyl sodium (16643-09-7) → norbornene (279-23-2) + bicyclo{2.2.1}hept-1-yltrimethylstannane (42204-95-5)

Guidance literature:

With dicyclohexylphosphane; In tetrahydrofuran; for 2h; Product distribution; Mechanism; Ambient temperature; other trapping agents or none, other solvents, other time;

DOI:10.1021/jo00085a012

upstream raw materials:

1-bromonorbornane

trimethylstannyl sodium

1-iodonorbornane

Refernces