N-<3-Thiapropyl>-5-phenyl-4,5-dithiapentanamid-disulfid

Base Information

• Chemical Name: N-<3-Thiapropyl>-5-phenyl-4,5-dithiapentanamid-disulfid
• CAS No.: 3312-99-0
• Molecular Formula: C₂₂H₂₈N₂O₂S₆
• Molecular Weight: 544.873
• Mol file: 3312-99-0.mol

Synonyms:N-<3-Thiapropyl>-5-phenyl-4,5-dithiapentanamid-disulfid

Chemical Property of N-<3-Thiapropyl>-5-phenyl-4,5-dithiapentanamid-disulfid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-<3-Thiapropyl>-5-phenyl-4,5-dithiapentanamid-disulfid

There total 3 articles about N-<3-Thiapropyl>-5-phenyl-4,5-dithiapentanamid-disulfid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-Tritylthio-ethyl)-5-phenyl-4,5-dithiapentansaeureamid (3312-97-8) → N-<3-Thiapropyl>-5-phenyl-4,5-dithiapentanamid-disulfid (3312-99-0)

Guidance literature:

With thiocyanogen; boron trifluoride diethyl etherate; In ethyl acetate;

DOI:10.1021/ja01095a032

Reference yield:

3-phenyldithio-propanoic acid (3312-96-7) → N-<3-Thiapropyl>-5-phenyl-4,5-dithiapentanamid-disulfid (3312-99-0)

Guidance literature:

Multi-step reaction with 2 steps

1: DCC / CH₂Cl₂

2: (SCN)2, BF₃-Et₂O / ethyl acetate

With thiocyanogen; boron trifluoride diethyl etherate; dicyclohexyl-carbodiimide; In dichloromethane; ethyl acetate;

DOI:10.1021/ja01095a032

Reference yield:

N-(2-Benzhydrylthio-ethyl)-(5-phenyl-4,5-dithia-pentan)-saeureamid (15515-60-3) → N-<3-Thiapropyl>-5-phenyl-4,5-dithiapentanamid-disulfid (3312-99-0)

Guidance literature:

With thiocyanogen; acetic acid; trifluoroacetic acid; In ethyl acetate;

DOI:10.1016/S0040-4020(01)97902-5

upstream raw materials:

N-(2-Tritylthio-ethyl)-5-phenyl-4,5-dithiapentansaeureamid

N-(2-Benzhydrylthio-ethyl)-(5-phenyl-4,5-dithia-pentan)-saeureamid

3-phenyldithio-propanoic acid