2-chloro-2'-methoxy-5-nitrobenzophenone

Base Information

• Chemical Name: 2-chloro-2'-methoxy-5-nitrobenzophenone
• CAS No.: 173736-11-3
• Molecular Formula: C₁₄H₁₀ClNO₄
• Molecular Weight: 291.691
• Mol file: 173736-11-3.mol

Synonyms:2-chloro-2'-methoxy-5-nitrobenzophenone

Chemical Property of 2-chloro-2'-methoxy-5-nitrobenzophenone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-chloro-2'-methoxy-5-nitrobenzophenone

There total 5 articles about 2-chloro-2'-methoxy-5-nitrobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromoanisole (578-57-4) + 2-chloro-5-nitrobenzoylchloride (25784-91-2) → 2-chloro-2'-methoxy-5-nitrobenzophenone (173736-11-3)

Guidance literature:

With n-butyllithium; Zinc chloride; tetrakis(triphenylphosphine)palladium ⁽⁰⁾; In tetrahydrofuran; diethyl ether;

Reference yield:

2-chloro-2'-methoxy-5-nitrobenzhydrol (173736-10-2) → 2-chloro-2'-methoxy-5-nitrobenzophenone (173736-11-3)

Guidance literature:

With chromium(VI) oxide; In water; acetic acid; at 25 - 35 ℃; for 1h;

Reference yield:

tetrakis(triphenylphosphine) palladium(0) (14221-01-3) + 2-bromoanisole (578-57-4) + 2-chloro-5-nitrobenzoylchloride (25784-91-2) → 2-chloro-2'-methoxy-5-nitrobenzophenone (173736-11-3)

Guidance literature:

With n-butyllithium; Zinc chloride; In tetrahydrofuran; diethyl ether;

upstream raw materials:

2-chloro-2'-methoxy-5-nitrobenzhydrol

chromium(VI) oxide

2-bromoanisole

2-chloro-5-nitrobenzoylchloride

Downstream raw materials:

oxime of 2-chloro-2'-methoxy-5-nitrobenzophenone

Refernces

• 1、 -. "Processes and intermediate compounds for the preparation of 2-(N,N-disubstituted) amino-4-(perfluoroalkyl)-1, 3- oxazin-6-one and 6-(perfluoroalkyl) uracil compounds". . . Retrieved 2008/06/13.
• 2、 -. "Process for the preparation of 6-(perfluoroalkyl) uracil compounds from 2-(N,N-disubstituted) amino-4-(perfluoroalkyl)-1,3-oxazin-6-one compounds". . . Retrieved 2008/06/13.