C₂₄H₁₆N₆O₂S₄

Base Information

• Chemical Name: C₂₄H₁₆N₆O₂S₄
• CAS No.: 1430236-05-7
• Molecular Formula: C₂₄H₁₆N₆O₂S₄
• Molecular Weight: 548.694
• Mol file: 1430236-05-7.mol

Synonyms:C₂₄H₁₆N₆O₂S₄

Chemical Property of C₂₄H₁₆N₆O₂S₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₁₆N₆O₂S₄

There total 5 articles about C₂₄H₁₆N₆O₂S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

2-chloro-N-(6-thiocyanatobenzo[d]thiazol-2-yl)acetamide (1338431-88-1) + C14H11N3OS2 (1430235-98-5) → C24H16N6O2S4 (1430236-05-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 - 105 ℃; for 12h;

DOI:10.1016/j.ejmech.2012.12.055

Reference yield:

2-benzylsulfanylnicotinic acid methyl ester → C24H16N6O2S4 (1430236-05-7)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrazine hydrate / methanol / 5 h / Reflux

2: carbon disulfide; potassium hydroxide / methanol / 5 h / Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 12 h / 100 - 105 °C

With carbon disulfide; hydrazine hydrate; potassium carbonate; potassium hydroxide; In methanol; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2012.12.055

Reference yield:

2-benzylsulfanyl-nicotinic acid hydrazide (1334647-18-5) → C24H16N6O2S4 (1430236-05-7)

Guidance literature:

Multi-step reaction with 2 steps

1: carbon disulfide; potassium hydroxide / methanol / 5 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 100 - 105 °C

With carbon disulfide; potassium carbonate; potassium hydroxide; In methanol; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2012.12.055

upstream raw materials:

2-chloro-N-(6-thiocyanatobenzo[d]thiazol-2-yl)acetamide

C₁₄H₁₁N₃OS₂

2-benzylsulfanyl-nicotinic acid hydrazide

2-benzylsulfanylnicotinic acid

Refernces