Technology Process of 3-(9H-carbazol-9-yl)phenyl boronic acid
There total 4 articles about 3-(9H-carbazol-9-yl)phenyl boronic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
ethanol; water; toluene;
for 5h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(l) iodide; potassium phosphate; ethylenediamine / toluene / 24 h / 120 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C
2.2: 2 h
3.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; ethanol / 24 h / 120 °C
With
potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; sodium carbonate; ethylenediamine;
In
tetrahydrofuran; ethanol; hexane; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C
1.2: 2 h
2.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; ethanol / 24 h / 120 °C
With
tetrakis(triphenylphosphine) palladium(0); n-butyllithium; sodium carbonate;
In
tetrahydrofuran; ethanol; hexane; toluene;
