potassium diethyldithiocarbamate

Base Information

• Chemical Name: potassium diethyldithiocarbamate
• CAS No.: 3699-30-7
• Molecular Formula: C5H10KNS2
• Molecular Weight: 187.371
• Mol file: 3699-30-7.mol

Synonyms:

Chemical Property of potassium diethyldithiocarbamate

Chemical Property:

• Boiling Point: 176.4°Cat760mmHg
• Flash Point: 60.5°C
• Density: 1.086g/cm³

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of potassium diethyldithiocarbamate

There total 1 articles about potassium diethyldithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + diethylamine (109-89-7) → potassium diethyldithiocarbamate (3699-30-7)

Guidance literature:

With potassium hydroxide; In water; for 1.5h;

DOI:10.1039/DT9920001477

Reference yield: 92.0%

potassium diethyldithiocarbamate (3699-30-7) + 2-Chloro-2-phenyl-N-(5-phenyl-[1,3,4]oxadiazol-2-yl)-acetamide (199338-97-1) → diethyl-dithiocarbamic acid phenyl-(5-phenyl-[1,3,4]oxadiazol-2-ylcarbamoyl)-methyl ester

Guidance literature:

In ethanol; for 1h; Heating;

DOI:10.1016/S0014-827X(98)00063-9

Reference yield: 87.0%

potassium diethyldithiocarbamate (3699-30-7) + N-(3-methylthiophenyl)-N-chloroacetylphenylamine (255367-48-7) → diethyl-dithiocarbamic acid [(3-methylsulfanyl-phenyl)-phenyl-carbamoyl]-methyl ester

Guidance literature:

In ethanol; for 1h; Heating;

DOI:10.1002/(SICI)1521-4184(199912)332:12<422::AID-ARDP422>3.0.CO;2-0

upstream raw materials:

carbon disulfide

diethylamine

Downstream raw materials:

DL-<(Diethylamino)thioxomethylthio>phenylessigsaeure

N,N-diethyl-2,2-diphenylacetamide

(N,N-diethylthiocarbamoylthio)acetic acid

C₁₉H₂₀ClNOS₂

Refernces

• 1、 El-Nassan, Hala Bakr. "Synthesis and antitumor activity of tetrahydrocarbazole hybridized with dithioate derivatives". . p. 308 - 315. Retrieved 2015/04/14.
• 2、 Kapanda, Coco N.,Muccioli, Giulio G.,Labar, Geoffray,Poupaert, Jacques H.,Lambert, Didier M.. "Bis(dialkylaminethiocarbonyl)disulfides as potent and selective monoglyceride lipase inhibitors". experimental part. p. 7310 - 7314. Retrieved 2010/07/14.