4-amino-3,5-dinitrobenzenesulfonyl chloride

Base Information

• Chemical Name: 4-amino-3,5-dinitrobenzenesulfonyl chloride
• CAS No.: 42760-43-0
• Molecular Formula: C₆H₄ClN₃O₆S
• Molecular Weight: 281.633
• Mol file: 42760-43-0.mol

Synonyms:4-amino-3,5-dinitrobenzenesulfonyl chloride

Chemical Property of 4-amino-3,5-dinitrobenzenesulfonyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-amino-3,5-dinitrobenzenesulfonyl chloride

There total 7 articles about 4-amino-3,5-dinitrobenzenesulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

ethyl 4-(chlorosulfonyl)phenylcarbamate (21208-62-8) → 4-amino-3,5-dinitrobenzenesulfonyl chloride (42760-43-0) + ethyl<(4-chlorosulfonyl-2-nitro)phenyl>carbamate (84202-48-2)

Guidance literature:

With sodium nitrate; sulfuric acid; for 20h; Ambient temperature;

Reference yield: 17.0%

p-acetylaminobenzenesulfonyl chloride (121-60-8) → 4-amino-3,5-dinitrobenzenesulfonyl chloride (42760-43-0) + 4-acetylamino-3-nitro-benzenesulphonyl chloride (16761-19-6)

Guidance literature:

With sodium nitrate; sulfuric acid; at 0 - 5 ℃; for 3h;

Reference yield:

→ 4-amino-3,5-dinitrobenzenesulfonyl chloride (42760-43-0)

Guidance literature:

With phosphorus pentachloride; trichlorophosphate;

DOI:10.1021/ja01626a055

upstream raw materials:

4-Chloro-3,5-dinitrobenzenesulphonyl Chloride

ethyl 4-(chlorosulfonyl)phenylcarbamate

p-acetylaminobenzenesulfonyl chloride

potassium 4-amino-3,5-dinitrobenzenesulfonate

Downstream raw materials:

5-methylsulfanyl-benzene-1,2,3-triyltriamine

3.5-Dinitro-sulfanilylhydrazid

3,4,5-triamino-thiophenol

Refernces

• 1、 -. "ORGANIC COMPOUND, CRYSTAL DIELECTRIC LAYER AND CAPACITOR BACKGROUND". Page/Page column 20; 21; 22; 23; 24; 25. . Retrieved 2017/05/10.
• 2、 George, Tesmol G.,Johnsamuel, Jayaseharan,Delfin, Dawn A.,Yakovich, Adam,Mukherjee, Mitali,Phelps, Mitch A.,Dalton, James T.,Sackett, Dan L.,Kaiser, Marcel,Brun, Reto,Werbovetz, Karl A.. "Antikinetoplastid antimitotic activity and metabolic stability of dinitroaniline sulfonamides and benzamides". . p. 5699 - 5710. Retrieved 2007/10/03.