Technology Process of C38H42N10O2
There total 7 articles about C38H42N10O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; bathophenanthrolinedispufonic acid disodium salt; sodium L-ascorbate;
In
water; tert-butyl alcohol;
at 110 ℃;
for 0.25h;
Microwave irradiation;
DOI:10.1016/j.bmcl.2012.07.009
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / tetrahydrofuran / 2.5 h / 4 - 20 °C
1.2: 20 °C
2.1: hydrogen; 10% Pd/C / tetrahydrofuran / 20 °C
3.1: hydrogenchloride; tert.-butylnitrite / tetrahydrofuran; water / 1.5 h / 4 °C
3.2: 4 - 20 °C
4.1: bathophenanthrolinedispufonic acid disodium salt; copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 0.25 h / 110 °C / Microwave irradiation
With
hydrogenchloride; tert.-butylnitrite; copper(ll) sulfate pentahydrate; 10% Pd/C; bathophenanthrolinedispufonic acid disodium salt; hydrogen; sodium L-ascorbate; triethylamine;
In
tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2012.07.009
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen; 10% Pd/C / tetrahydrofuran / 20 °C
2.1: hydrogenchloride; tert.-butylnitrite / tetrahydrofuran; water / 1.5 h / 4 °C
2.2: 4 - 20 °C
3.1: bathophenanthrolinedispufonic acid disodium salt; copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 0.25 h / 110 °C / Microwave irradiation
With
hydrogenchloride; tert.-butylnitrite; copper(ll) sulfate pentahydrate; 10% Pd/C; bathophenanthrolinedispufonic acid disodium salt; hydrogen; sodium L-ascorbate;
In
tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2012.07.009