Technology Process of 3-hexyl-1-(2',7'-dibromo-9',9'-diphenylfluoren-4'-yl)nonan-1-one
There total 6 articles about 3-hexyl-1-(2',7'-dibromo-9',9'-diphenylfluoren-4'-yl)nonan-1-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-hexyl-1-octylzinc bromide;
With
copper(l) cyanide; lithium chloride;
In
tetrahydrofuran;
for 0.25h;
Cooling with ice;
C26H15Br2ClO;
In
tetrahydrofuran;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrahydrofuran; dibutyl ether / 2 h / -78 - 20 °C / Inert atmosphere
2.1: trifluoroacetic acid / chlorobenzene / 48 h / Reflux
3.1: thionyl chloride / toluene / 24 h / Inert atmosphere; Reflux
4.1: lithium chloride; copper(l) cyanide / tetrahydrofuran / 0.25 h / Cooling with ice
4.2: 20 °C
With
thionyl chloride; copper(l) cyanide; trifluoroacetic acid; lithium chloride;
In
tetrahydrofuran; dibutyl ether; chlorobenzene; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / chlorobenzene / 48 h / Reflux
2.1: thionyl chloride / toluene / 24 h / Inert atmosphere; Reflux
3.1: lithium chloride; copper(l) cyanide / tetrahydrofuran / 0.25 h / Cooling with ice
3.2: 20 °C
With
thionyl chloride; copper(l) cyanide; trifluoroacetic acid; lithium chloride;
In
tetrahydrofuran; chlorobenzene; toluene;