Technology Process of C41H54O2S2Si3
There total 4 articles about C41H54O2S2Si3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis(acetylacetonate)nickel(II); diisobutylaluminium hydride; triethylphosphine;
In
tetrahydrofuran; cyclohexane;
at 80 ℃;
for 10h;
DOI:10.1021/ja00040a063
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 54 percent / LAH / diethyl ether
2: 95 percent / Et3N, DMAP / CH2Cl2
3: 96 percent / PdCl2(PPh3)2, CuI, Et2NH
4: 40 percent / Ni(acac)2, PEt3, DIBAH / cyclohexane; tetrahydrofuran / 10 h / 80 °C
With
dmap; bis-triphenylphosphine-palladium(II) chloride; bis(acetylacetonate)nickel(II); copper(l) iodide; lithium aluminium tetrahydride; diisobutylaluminium hydride; diethylamine; triethylamine; triethylphosphine;
In
tetrahydrofuran; diethyl ether; dichloromethane; cyclohexane;
DOI:10.1021/ja00040a063
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 95 percent / Et3N, DMAP / CH2Cl2
2: 96 percent / PdCl2(PPh3)2, CuI, Et2NH
3: 40 percent / Ni(acac)2, PEt3, DIBAH / cyclohexane; tetrahydrofuran / 10 h / 80 °C
With
dmap; bis-triphenylphosphine-palladium(II) chloride; bis(acetylacetonate)nickel(II); copper(l) iodide; diisobutylaluminium hydride; diethylamine; triethylamine; triethylphosphine;
In
tetrahydrofuran; dichloromethane; cyclohexane;
DOI:10.1021/ja00040a063