4,4'-di-tert-octyldiphenylnitrosoamine

Base Information

• Chemical Name: 4,4'-di-tert-octyldiphenylnitrosoamine
• CAS No.: 84077-82-7
• Molecular Formula: C₂₈H₄₂N₂O
• Molecular Weight: 422.654
• Mol file: 84077-82-7.mol

Synonyms:4,4'-di-tert-octyldiphenylnitrosoamine

Chemical Property of 4,4'-di-tert-octyldiphenylnitrosoamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,4'-di-tert-octyldiphenylnitrosoamine

There total 1 articles about 4,4'-di-tert-octyldiphenylnitrosoamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine (15721-78-5) → 4,4'-di-tert-octyldiphenylnitrosoamine (84077-82-7)

Guidance literature:

With hydrogenchloride; sodium nitrite; In ethanol; isopropyl alcohol; at 0 - 5 ℃; for 1h;

DOI:10.1016/0022-2364(82)90057-9

Reference yield:

4,4'-di-tert-octyldiphenylnitrosoamine (84077-82-7) → 1,1-di-(4-tert-octylphenyl)hydrazine

Guidance literature:

With acetic acid; zinc; In isopropyl alcohol; at 20 - 25 ℃; for 3.5h;

DOI:10.1016/0022-2364(82)90057-9

Reference yield:

4,4'-di-tert-octyldiphenylnitrosoamine (84077-82-7) → 2,2-di(4-tert-octylphenyl)-1-picrylhydrazyl, free radical (84077-81-6)

Guidance literature:

Multi-step reaction with 3 steps

1: Zn, AcOH / propan-2-ol / 3.5 h / 20 - 25 °C

2: sodium bicarbonate / propan-2-ol / 0.5 h / Heating

3: 74 percent / PbO₂, Na₂SO₄ / CHCl₃ / 1 h / 25 °C

With sodium hydrogencarbonate; lead dioxide; acetic acid; sodium sulfate; zinc; In chloroform; isopropyl alcohol;

DOI:10.1016/0022-2364(82)90057-9

upstream raw materials:

di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine

Downstream raw materials:

2,2-di(4-tert-octylphenyl)-1-picrylhydrazyl, free radical

Refernces